Understanding Calibration
What is Calibration?
Calibration is the process of comparing your instrument's measurements to known standard values. It's like using a ruler to check if your measuring tape is accurate - but for laboratory instruments.
Why Multi-point Calibration?
Multi-point calibration offers several advantages over single-point calibration:
- Verifies linearity across your method's entire measuring range
- Identifies systematic errors at different concentrations
- Provides more reliable results across different concentration levels
- Meets regulatory requirements for method validation
Thompson, M. & Ellison, S. L. R. Fitness for purpose of analytical methods: A laboratory guide to method validation and related topics. Eurachem Guide (2014).
Calculator
Results
Standard Value |
Measured Value |
Absolute Difference |
Relative Difference (%) |
Bias |
Interpreting Your Results
Key Parameters
- Slope: Should be close to 1.0 for a well-calibrated system. Significant deviation suggests proportional bias.
- Y-intercept: Should be close to 0. Deviation indicates constant bias.
- R²: Measures linearity. Values closer to 1.0 indicate better linearity.
Acceptance Criteria
Common acceptance criteria include:
- R² ≥ 0.995 for most analytical methods
- Relative difference typically ≤ 10% at each level
- Slope between 0.9 and 1.1
- Y-intercept not significantly different from zero
ISO/IEC 17025:2017 General requirements for the competence of testing and calibration laboratories